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HRID 53853생성일: 2026년 10월 24일

2,6-Di-tert-butyl-4-(2-nitrostyryl)phenol → 4-(2-Aminophenethyl)-2,6-di-tert-butylphenol

https://huagongshe.com/ko/reaction/53853

반응식

참여 물질

역할이름HCID투입량
반응물2,6-Di-tert-butyl-4-(2-nitrostyryl)phenolHCID 54141749—
촉매HCID 178418390HCID 178418390—
용매EthanolHCID 702—
생성물4-(2-Aminophenethyl)-2,6-di-tert-butylphenolHCID 19960469199.1%

반응 단계

To a suspension of 2,6-di-tert-butyl-4-(2-nitrostyryl)phenol (16.4 g, 23.3 mmol) in ethanol (150 ml) was added a catalytic amount of 10% palladium carbon and the suspension was subjected to catalytic reduction at room temperature at 1-2.5 atms for 8 hrs and at 40° C. for 3 hrs. After filtering the catalyst, distilling off the solvent gave 4-(2-aminophenethyl)-2,6-di-tert-butylphenol (15.1 g, 100%) as a viscous oil.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05621010
출처 데이터셋uspto-grants-1997_04
ORD IDord-7132e3607c4742b892cc59832a2db099
출처 메모uspto-grants-1997_04