Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl formate → Benzyl [3-(formylamino)propyl]carbamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl formate | HCID 8025 | — |
| 반응물 | Benzyl (3-aminopropyl)carbamate | HCID 417669 | — |
| 생성물 | Benzyl [3-(formylamino)propyl]carbamate | HCID 86691669 | 99% |
반응 단계
Benzyl 3-aminopropylcarbamate 12 (8.00 g, 36.0 mmol) was dissolved in 250 mL of ethyl formate. The solution was refluxed for 4 h. Following complete conversion of the amine, the solution was concentrated to dryness in a rotary evaporator to obtain the formamide as a colorless oil (8.90 g, 99%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08865863B2 |
| 출처 데이터셋 | uspto-grants-2014_10 |
| ORD ID | ord-e07e3cc5e80d4db8abe3016866640096 |
| 출처 메모 | uspto-grants-2014_10 |