Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonia → 1,1-Cyclohexanedicarboxamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | Cyclohexane-1,1-dicarboxylic acid | HCID 136906 | — |
| 반응물 | 1,1-Cyclohexanedicarboxamide | HCID 299204 | — |
| 생성물 | 1,1-Cyclohexanedicarboxamide | HCID 299204 | — |
| 생성물 | 1,1-Cyclohexanedicarbonitrile | HCID 544561 | — |
반응 단계
Furthermore, as a method for producing bis(aminomethyl)cyclohexane, for example, Non-Patent Document 1 (Malachowski et al.) discloses the following: an acid chloride derivative is prepared using cyclohexanedicarboxylic acid with thionyl chloride; cyclohexane diamide is prepared using the acid chloride derivative with ammonia; and thereafter, the cyclohexane diamide is further allowed to react with thionyl chloride to obtain dicyanocyclohexane, and then the obtained dicyanocyclohexane is hydrogenated.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08865938B2 |
| 출처 데이터셋 | uspto-grants-2014_10 |
| ORD ID | ord-17d89f5f75154560a35f326706e8dd50 |
| 출처 메모 | uspto-grants-2014_10 |