반응식
C1[CH:5]2[CH:6]3[CH:10]=[CH:9][CH:8]([CH:4]2[CH:3]=C1)[CH2:7]3.C([OH:14])C=C>>[CH:8]12[CH2:7][CH:6]([CH:10]=[CH:9]1)[CH2:5][CH:4]2[CH2:3][OH:14]참가 물질
3
반응 조건
- 온도
- 210 °C
실험 절차
397 g (3 mol) of dicyclopentadiene (DCPD) (produced from Aldrich Inc.) and 331 g (5.7 mol) of allyl alcohol (produced from Aldrich Inc.) were added to a 2 L high-pressure reactor and the temperature of the 2 L high-pressure reactor was increased to 210° C. The resulting mixture was reacted for one hour, stirring at 300 rpm. When the reaction was completed, the reactant was cooled and loaded into a distillation device. The reactant was distilled twice at a reduced pressure of 1 torr using a vacuum pump to attain a product at 56° C. (Yield: 52%).
후처리
- customThe resulting mixture was reacted for one hour
- temperaturethe reactant was cooled
- distillationThe reactant was distilled twice at a reduced pressure of 1 torr
- customat 56° C.
출처 및 근거
- ORD 기록
- ord-20fe3722c4d54d728a127692cca28ede
- 출처 데이터셋
- uspto-grants-2014_10
- 특허 번호
- USRE045219E1
연결된 노트
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