Ethyl isocyanate → HCID 136197293, 화합물

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[OH:1][C:2]1[CH:3]=[CH:4][C:5]([O:19][CH2:20][CH2:21][CH3:22])=[C:6]([C:8]2[NH:13][C:12](=[O:14])[C:11]([CH2:15][CH3:16])=[C:10]([CH2:17][CH3:18])[N:9]=2)[CH:7]=1.[CH2:23]([N:25]=[C:26]=[O:27])[CH3:24]>>[CH2:23]([NH:25][C:26]([O:1][C:2]1[CH:3]=[CH:4][C:5]([O:19][CH2:20][CH2:21][CH3:22])=[C:6]([C:8]2[NH:13][C:12](=[O:14])[C:11]([CH2:15][CH3:16])=[C:10]([CH2:17][CH3:18])[N:9]=2)[CH:7]=1)=[O:27])[CH3:24]

참가 물질

반응물 2

HCID 8022Ethyl isocyanate

HCID 136197392HCID 136197392, 화합물

생성물 1

HCID 136197293HCID 136197293, 화합물

실험 절차

The title compound was prepared by reacting the compound of example 81 with ethyl isocyanate in the same manner as that of example 35. 1H NMR (CDCl3) δ: 8.20 (1H, d), 7.25 (1H, dd), 6.99 (1H, d), 5.06 (1H, br), 4.14 (2H, t), 3.32 (2H, m), 2.66 (2H, q), 2.58 (2H, q), 1.98 (2H, m), 1.28 (3H, t), 1.22 (3H, t), 1.14 (3H, t), 1.13 (3H, t).

출처 및 근거

ORD 기록: ord-69fcb36af676496f842ac6562cae76a9
출처 데이터셋: uspto-grants-2014_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08871777B2

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