Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl 2-iodo-4-nitrobenzoate → Methyl 2-({3-[(tert-butoxycarbonyl)amino]phenyl}ethynyl)-4-nitrobenzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl 2-iodo-4-nitrobenzoate | HCID 232745 | — |
| 반응물 | tert-Butyl 3-ethynylphenylcarbamate | HCID 11275982 | — |
| 생성물 | Methyl 2-({3-[(tert-butoxycarbonyl)amino]phenyl}ethynyl)-4-nitrobenzoate | HCID 57961859 | 87% |
반응 단계
This compound was prepared according to the procedure of Example B19 step C, using tert-butyl (3-ethynylphenyl)carbamate and methyl 2-iodo-4-nitrobenzoate as the starting materials in 87% yield. LCMS calculated for C21H21N2O6(M+H)+: m/z=397.1.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08871753B2 |
| 출처 데이터셋 | uspto-grants-2014_10 |
| ORD ID | ord-6f507852724743249a63560f1d1103b7 |
| 출처 메모 | uspto-grants-2014_10 |