3-Difluoromethoxy-2-nitrotoluene → 2-(Difluoromethoxy)-6-methylaniline

HRID 542654

반응식

HRID 542654 반응식
[F:1][CH:2]([F:14])[O:3][C:4]1[C:5]([N+:11]([O-])=O)=[C:6]([CH3:10])[CH:7]=[CH:8][CH:9]=1>C(O)C>[F:1][CH:2]([F:14])[O:3][C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([CH3:10])[C:5]=1[NH2:11]

참가 물질

3

반응물 1

HCID 189816253-Difluoromethoxy-2-nitrotoluene

생성물 1

HCID 189816732-(Difluoromethoxy)-6-methylaniline수율 95%

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

The procedures of Example 2 were repeated except that the starting material was 16.0 g (79 mmol) of 3-difluoromethoxy-2-nitrotoluene as dissolved in 100 ml of ethanol. As a result, 13.0 g of 2-difluoromethoxy-6-methyl aniline was obtained.

출처 및 근거

ORD 기록
ord-d9c6221693334c679788aeadd6e9a575
출처 데이터셋
uspto-grants-1987_04
특허 번호
US04659365

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