Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzoyl Peroxide → 1-Bromo-3-(bromomethyl)-5-methoxybenzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzoyl Peroxide | HCID 7187 | — |
| 반응물 | N-bromobutanimide | HCID 67184 | — |
| 반응물 | 1-Bromo-3-methoxy-5-methylbenzene | HCID 10679554 | — |
| 용매 | Carbon Tetrachloride | HCID 5943 | — |
| 생성물 | 1-Bromo-3-(bromomethyl)-5-methoxybenzene | HCID 12276449 | — |
반응 단계
A mixture of 5-bromo-3-methoxytoluene (20 g, 0.1 m), N-bromosuccinimide (17.8 g, 0.1 m) and dibenzoyl peroxide in carbon tetrachloride (200 ml) is heated to reflux and irradiated with a sunlamp. The mixture is cooled, filtered and concentrated in vacuo to give 5-bromo-3-methoxybenzyl bromide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04659706 |
| 출처 데이터셋 | uspto-grants-1987_04 |
| ORD ID | ord-a4d130a503364d3fa2710805bc0d4325 |
| 출처 메모 | uspto-grants-1987_04 |