Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Aniline → 3-(4-methoxyphenyl)-4-phenyl-5-methyl-4H-1,2,4-triazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Aniline | HCID 6115 | — |
| 반응물 | Phosphorus trichloride | HCID 24387 | — |
| 반응물 | N'-acetyl-4-methoxybenzohydrazide | HCID 839858 | — |
| 용매 | 1,2-Dichlorobenzene | HCID 7239 | — |
| 생성물 | 3-(4-methoxyphenyl)-4-phenyl-5-methyl-4H-1,2,4-triazole | HCID 13054023 | — |
반응 단계
Using the procedure of Step B in Example 1, 26.3 ml of aniline, 150 ml of o-dichlorobenzene, 4.65 ml of phosphorus trichloride and 10 g of N-(4-methoxybenzoyl)-N'-acetyl-hydrazine [prepared by process of J. Org., Vol. 19 (1954), p. 194-201] were reacted to obtain 7.1 g of 3-(4-methoxyphenyl)-4-phenyl-5-methyl-4H-1,2,4-triazole melting at 140°-141° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04659729 |
| 출처 데이터셋 | uspto-grants-1987_04 |
| ORD ID | ord-37d150b3944448f189500d67a146a3b8 |
| 출처 메모 | uspto-grants-1987_04 |