Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → Hexadecyl-ammoniumethyl phosphonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Hexadecylamine | HCID 8926 | — |
| 반응물 | Diethylphosphite | HCID 3780918 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Hexadecyl-ammoniumethyl phosphonate | HCID 20196053 | 97% |
반응 단계
To a mixture of 34.6 g. (0.25 moles) of diethyl phosphite, 50 ml. of water and 50 ml. of ethanol 60.4 g (0.25 moles) of hexadecyl amine and 70 ml. of ethanol are added. The reaction mixture is refluxed for 4 hours, whereupon the solvent is distilled off in vacuo. 85.2 g. of hexadecyl-ammoniumethyl phosphonate are obtained. Yield: 97.0%. Melting point: 50° to 52° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04661477 |
| 출처 데이터셋 | uspto-grants-1987_04 |
| ORD ID | ord-30df575a8f8f4b72a3113d20d10f4013 |
| 출처 메모 | uspto-grants-1987_04 |