Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Resorcinol → 7-(2,4-Dihydroxyphenyl)-3,7-dimethyloct-1-yl acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Resorcinol | HCID 5054 | — |
| 반응물 | p-Toluenesulfonic acid | HCID 6101 | — |
| 반응물 | Citronellyl Acetate | HCID 9017 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | 7-(2,4-Dihydroxyphenyl)-3,7-dimethyloct-1-yl acetate | HCID 20206138 | — |
반응 단계
11.0 Parts of resorcinol, 10.0 parts of citronellyl acetate and 0.5 parts of p-toluene sulphonic acid are heated at 115° C. for 45 hours. The reaction mixture is then taken up in ether, washed with sodium bicarbonate solution, water, and evaporated. The residual oil is distilled and yields 3.9 parts of 7-(2',4'-dihydroxyphenyl)-3,7-dimethyloct-1-yl acetate b0.2 215° C. with the following percentage composition by weight:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04661601 |
| 출처 데이터셋 | uspto-grants-1987_04 |
| ORD ID | ord-b8b1ed0b9d3a47e191277d737c1ec4a1 |
| 출처 메모 | uspto-grants-1987_04 |