Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → 2-Propenoic acid, 3-(4-chlorophenyl)-, ethyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | Styrene | HCID 7501 | — |
| 반응물 | 4-Chlorostyrene | HCID 14085 | — |
| 촉매 | Palladium Chloride | HCID 24290 | — |
| 생성물 | 2-Propenoic acid, 3-(4-chlorophenyl)-, ethyl ester | HCID 201471 | 60.2% |
반응 단계
The procedures of Example 27 were exactly followed except that p-chlorostyrene and ethanol were used respectively instead of styrene and methanol and the amount of palladium chloride was changed to 0.1 millimole. Ethyl 4-chlorocinnamate was obtained with a yield of 60.2%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04661620 |
| 출처 데이터셋 | uspto-grants-1987_04 |
| ORD ID | ord-6f402cd1951d44a9b4643cffbe16cf59 |
| 출처 메모 | uspto-grants-1987_04 |