Hexamethylenetetramine → HCID 20206374, 화합물

HRID 543390노트

반응식

HRID 543390 반응식
Cl.N[CH2:3][C:4]1[C:12]([OH:13])=[C:11]([S:14]([CH3:17])(=[O:16])=[O:15])[CH:10]=[C:9]2[C:5]=1[CH2:6][CH2:7][CH2:8]2.C1N2CN3CN(C2)CN1C3.FC(F)(F)C(O)=[O:31]>>[CH:3]([C:4]1[C:12]([OH:13])=[C:11]([S:14]([CH3:17])(=[O:16])=[O:15])[CH:10]=[C:9]2[C:5]=1[CH2:6][CH2:7][CH2:8]2)=[O:31]

참가 물질

4

반응물 3

HCID 4101HexamethylenetetramineHCID 6422Trifluoroacetic acidHCID 20206375HCID 20206375, 화합물

생성물 1

HCID 20206374HCID 20206374, 화합물

실험 절차

0.83 g (0.003 mol) of 4-aminomethyl-5-hydroxy-6-methylsulfonylindane hydrochloride is reacted with 0.42 g of urotropine in 6 ml of trifluoroacetic acid in analogy to Example 1. Melting point: 152°-153° C.

출처 및 근거

ORD 기록
ord-b81630aa043f4b63a74a1e6453eb5ce7
출처 데이터셋
uspto-grants-1987_04
특허 번호
US04661636

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