Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Propenoic acid, 3-hydroxypropyl ester → Isopropenylphosphonic Acid Hydroxypropylacrylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Propenoic acid, 3-hydroxypropyl ester | HCID 33101 | — |
| 반응물 | Ammonium Persulfate | HCID 62648 | — |
| 반응물 | Peroxydisulfate | HCID 107879 | — |
| 반응물 | Isopropenylphosphonic acid | HCID 557541 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Isopropenylphosphonic Acid Hydroxypropylacrylate | HCID 86739384 | — |
반응 단계
Using the apparatus and methodology as described in Example 1, isopropenyl phosphonic acid (61.6 g, 54%, 0.27 mole), hydroxypropylacrylate (16.6 g, 0.13 mole) and water (121.8 g) were charged in the reactor. Ammonium persulfate (6 g) was added. After 11/2 hours of reflux, 6 g additional persulfate was added followed by an equivalent reflux period. The final pH of the yellow solution was 0.72.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04446028 |
| 출처 데이터셋 | uspto-grants-1984_05 |
| ORD ID | ord-5d4d50ba7f4644d680f84acc41bdccb2 |
| 출처 메모 | uspto-grants-1984_05 |