2-Propenoic acid, 3-hydroxypropyl ester → Isopropenylphosphonic Acid Hydroxypropylacrylate

HRID 543455

반응식

HRID 543455 반응식
[C:1]([P:4](=[O:7])([OH:6])[OH:5])([CH3:3])=[CH2:2].[OH:8][CH2:9][CH2:10][CH2:11][O:12][C:13](=[O:16])[CH:14]=[CH2:15]>O>[C:1]([P:4](=[O:5])([OH:7])[OH:6])([CH3:3])=[CH2:2].[OH:8][CH2:9][CH2:10][CH2:11][O:12][C:13](=[O:16])[CH:14]=[CH2:15]

참가 물질

4

반응물 2

HCID 331012-Propenoic acid, 3-hydroxypropyl esterHCID 557541Isopropenylphosphonic acid

생성물 1

HCID 86739384Isopropenylphosphonic Acid Hydroxypropylacrylate

시약·촉매·용매 1

HCID 962Water용매

실험 절차

Used the method of Example 5, isopropenyl phosphonic acid (30.7 g, 54%, 0.14 mole), hydroxypropylacrylate (36.4 g, 0.28 mole) and water (144.9 g) were charged in the reactor. The bulk of the polymer crystallized during the first period of reflux and was found to be insoluble in water.

후처리

  1. customThe bulk of the polymer crystallized during the first period
  2. temperatureof reflux

출처 및 근거

ORD 기록
ord-49e0e65a7ace49c29f56fbb104f02e73
출처 데이터셋
uspto-grants-1984_05
특허 번호
US04446028

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