2-Propenoic acid, 3-hydroxypropyl ester → Isopropenylphosphonic Acid Hydroxypropylacrylate
반응식
[C:1]([P:4](=[O:7])([OH:6])[OH:5])([CH3:3])=[CH2:2].[OH:8][CH2:9][CH2:10][CH2:11][O:12][C:13](=[O:16])[CH:14]=[CH2:15]>O>[C:1]([P:4](=[O:5])([OH:7])[OH:6])([CH3:3])=[CH2:2].[OH:8][CH2:9][CH2:10][CH2:11][O:12][C:13](=[O:16])[CH:14]=[CH2:15]참가 물질
4
실험 절차
Used the method of Example 5, isopropenyl phosphonic acid (30.7 g, 54%, 0.14 mole), hydroxypropylacrylate (36.4 g, 0.28 mole) and water (144.9 g) were charged in the reactor. The bulk of the polymer crystallized during the first period of reflux and was found to be insoluble in water.
후처리
- customThe bulk of the polymer crystallized during the first period
- temperatureof reflux
출처 및 근거
- ORD 기록
- ord-49e0e65a7ace49c29f56fbb104f02e73
- 출처 데이터셋
- uspto-grants-1984_05
- 특허 번호
- US04446028
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