Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Hydroxyethyl Methacrylate → Isopropenyl Phosphonic Acid Hydroxyethylmethacrylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Hydroxyethyl Methacrylate | HCID 13360 | — |
| 반응물 | Ammonium Persulfate | HCID 62648 | — |
| 반응물 | Isopropenylphosphonic acid | HCID 557541 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Isopropenyl Phosphonic Acid Hydroxyethylmethacrylate | HCID 86739386 | — |
반응 단계
Aqueous isopropenyl phosphonic acid (71 g, 54%, 0.3 mole) and hydroxyethylmethacrylate (13 g, 0.1 mole) were mixed with 121.6 g water in a resin kettle. Ammonium persulfate (6 g) was added. After 11/2 hours of reflux, an additional 6 g of initiator was added followed by another 11/2 hours of reflux. The final product was a yellow solution with a pH of 0.68. The 31PMR showed polymeric absorptions centered at δ=-29.5 and -24.3 ppm.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04446028 |
| 출처 데이터셋 | uspto-grants-1984_05 |
| ORD ID | ord-83e7242a4dca444995cd572292ecdc81 |
| 출처 메모 | uspto-grants-1984_05 |