Octylamine → HCID 178443600, 화합물

HRID 543662

반응식

HRID 543662 반응식
CS[C:3]1[N:8]=[C:7]([OH:9])[C:6]([C:10]([O:12][CH2:13][CH3:14])=[O:11])=[CH:5][N:4]=1.[CH2:15]([NH2:23])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]>C(O)C>[CH2:15]([NH:23][C:3]1[N:8]=[C:7]([OH:9])[C:6]([C:10]([O:12][CH2:13][CH3:14])=[O:11])=[CH:5][N:4]=1)[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]

참가 물질

4

반응물 2

HCID 8143OctylamineHCID 178418871HCID 178418871, 화합물

생성물 1

HCID 178443600HCID 178443600, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

2-Methylthio-5-ethoxycarbonyl-4-hydroxypyrimidine (2.5 mmol, 535 mg) was refluxed overnight in ethanol with n-octylamine (4 mmol, 650 μl). The product was filtered off and washed with ethanol. Yield 402 mg (54.5%)

후처리

  1. filtrationThe product was filtered off
  2. washwashed with ethanol

출처 및 근거

ORD 기록
ord-a7c6f1a861a84ac2bd25d0f91b70db8f
출처 데이터셋
uspto-grants-1984_05
특허 번호
US04447422

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