Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Lithium azide → 1-Azido-1-(5-chloro-2-pyridyl)-2-(1H-imidazol-1-yl)ethane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Lithium azide | HCID 88163 | — |
| 반응물 | 1-chloro-(5-chloro-2-pyridyl)-2-(1H-imidazol-1-yl)ethane | HCID 19959423 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 1-Azido-1-(5-chloro-2-pyridyl)-2-(1H-imidazol-1-yl)ethane | HCID 19959415 | — |
반응 단계
0.92 g of 1-chloro-(5-chloro-2-pyridyl)-2-(1H-imidazol-1-yl)ethane are added under argon to a solution of 0.37 g of lithium azide in 2 ml of dry dimethylformamide and the reaction mixture is stirred at 60° for 18 hours. Working up according to process A (see Example 1) gives the substance as a yellowish oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05622982 |
| 출처 데이터셋 | uspto-grants-1997_04 |
| ORD ID | ord-a1872d4c2faa42f194f06d6f8cbe80f7 |
| 출처 메모 | uspto-grants-1997_04 |