Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzene, 1-fluoro-2-methyl-4-nitro- → HCID 61151226, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzene, 1-fluoro-2-methyl-4-nitro- | HCID 68001 | — |
| 반응물 | Diisopropylethylamine | HCID 81531 | — |
| 반응물 | 1-(2-Ethoxyethyl)piperazine | HCID 2734643 | — |
| 용매 | Dimethyl Sulfoxide | HCID 679 | — |
| 생성물 | HCID 61151226 | HCID 61151226 | — |
반응 단계
In the same manner as in Production Example 5-1, but using 4-(2-ethoxyethyl)piperazine in place of N-ethylpiperazine used in Production Example 5-1, using 5-nitro-2-fluorotoluene in place of 2-fluoro-5-nitrobenzyl alcohol, using N,N-diisopropylethylamine in place of potassium carbonate, and using dimethylsulfoxide in place of N-methylpyrrolidone, the entitled compound was obtained as a yellow solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07935708B2 |
| 출처 데이터셋 | uspto-grants-2011_05 |
| ORD ID | ord-1118415f06c340358225aa91bac29e97 |
| 출처 메모 | uspto-grants-2011_05 |