HCID 57514842, 화합물 → 4-Piperidin-1-ylmethyl-phenol

HRID 547351

반응식

HRID 547351 반응식
[OH:1][C:2]1[CH:22]=[CH:21][C:5]([CH2:6][N:7]2[CH2:12][C@@H:11]3[CH2:13][C@H:8]2[CH2:9]N3C(OC(C)(C)C)=O)=[CH:4][CH:3]=1>C(Cl)Cl>[N:7]1([CH2:6][C:5]2[CH:4]=[CH:3][C:2]([OH:1])=[CH:22][CH:21]=2)[CH2:12][CH2:11][CH2:13][CH2:8][CH2:9]1

참가 물질

3

반응물 1

HCID 57514842HCID 57514842, 화합물

생성물 1

HCID 116369724-Piperidin-1-ylmethyl-phenol

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

The title compound was prepared using methods analogous to those described for Intermediate 35, substituting DCE for CH2Cl2. 1H NMR (500 MHz, CDCl3): 7.14-7.03 (m, 2H), 6.75 (br s, 1H), 6.62-6.53 (m, 2H), 3.41 (s, 2H), 2.49 (s, 4H), 1.66-1.59 (m, 4H), 1.50-1.42 (m, 2H). MS (ESI): mass calcd. for C12H17NO, 191.13; m/z found, 192.20 [M+H]+.

출처 및 근거

ORD 기록
ord-2d08a74c40b9466980c3fc8ec6b5ec6c
출처 데이터셋
uspto-grants-2011_05
특허 번호
US07939527B2

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