Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → N-[[(4-Nitrophenyl)methoxy]carbonyl]-L-isoleucine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | L-Isoleucine | HCID 6306 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Carbonic acid 4-Nitrophenyl (4-Nitrophenyl)methyl Ester | HCID 21829967 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | N-[[(4-Nitrophenyl)methoxy]carbonyl]-L-isoleucine | HCID 12184447 | 24.5% |
반응 단계
The title compound is prepared by the procedure of Example 255 using 14.73 g of product from Example 254, 6.07 g of L-isoleucine, 12.73 ml of triethylamine and 556 ml of 4:1 ethyl alcohol:water to give 3.52 g of the desired product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05623081 |
| 출처 데이터셋 | uspto-grants-1997_04 |
| ORD ID | ord-1849cdd34ca7460f86457d497ba7c0d0 |
| 출처 메모 | uspto-grants-1997_04 |