2-Thiopheneglyoxylic acid → 6-Nitro-3-thiophen-2-yl-1H-quinoxalin-2-one

HRID 548398

반응식

HRID 548398 반응식
[N+:1]([C:4]1[CH:5]=[C:6]([NH2:11])[C:7]([NH2:10])=[CH:8][CH:9]=1)([O-:3])=[O:2].[S:12]1[CH:16]=[CH:15][CH:14]=[C:13]1[C:17](=O)[C:18](O)=[O:19]>>[N+:1]([C:4]1[CH:5]=[C:6]2[C:7](=[CH:8][CH:9]=1)[NH:10][C:18](=[O:19])[C:17]([C:13]1[S:12][CH:16]=[CH:15][CH:14]=1)=[N:11]2)([O-:3])=[O:2]

참가 물질

3

실험 절차

The quinoxalin-2-one of the present example is prepared with 4-Nitro-benzene-1,2-diamine and (thiophen-2-yl) oxo-acetic acid via the method described in Example 12 to afford 6-Nitro-3-thiophen-2-yl-1H-quinoxalin-2-one.

출처 및 근거

ORD 기록
ord-4a169c6f04954c0e9e4cdf9a1c03f096
출처 데이터셋
uspto-grants-2011_05
특허 번호
USRE042375E1

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