Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrazine hydrate (1:1) → 4-(N-acetyl-N-phenylamino)butylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrazine hydrate (1:1) | HCID 24654 | — |
| 반응물 | N-[4-(N-acetyl-N-phenylamino)butyl]phthalimide | HCID 19956978 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 4-(N-acetyl-N-phenylamino)butylamine | HCID 19956980 | 80.7% |
반응 단계
A mixture of N-[4-(N-acetyl-N-phenylamino)butyl]phthalimide (9.2 g), hydrazine monohydrate (10 ml) and ethanol (200 ml) was heated under reflux for 1 hour. The deposited crystals were separated by filtration, and the filtrate was concentrated under reduced pressure to obtain 4-(N-acetyl-N-phenylamino)butylamine (4.55 g, 80.7%) as an oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05624917 |
| 출처 데이터셋 | uspto-grants-1997_04 |
| ORD ID | ord-31c993edd52c40a7b84d135cab1586bf |
| 출처 메모 | uspto-grants-1997_04 |