1-Bromo-4-(4-chlorostyryl)benzene → 3-Bromo-6-methoxyphenanthrene

HRID 549494노트

반응식

HRID 549494 반응식
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]=[CH:9][C:10]2[CH:15]=[CH:14][C:13]([O:16][CH3:17])=[CH:12][CH:11]=2)=[CH:4][CH:3]=1.BrC1C=CC(C=CC2C=CC(Cl)=CC=2)=CC=1>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]2[CH:8]=[CH:9][C:10]3[C:11]([C:6]=2[CH:7]=1)=[CH:12][C:13]([O:16][CH3:17])=[CH:14][CH:15]=3

참가 물질

3

반응물 2

HCID 539115281-Bromo-4-(4-chlorostyryl)benzeneHCID 541582251-Bromo-4-[2-(4-methoxyphenyl)ethenyl]benzene

생성물 1

HCID 866148773-Bromo-6-methoxyphenanthrene

실험 절차

This phenanthrene was prepared as described in Step 2 of Example 36, substituting 1-bromo-4-[2-(4-methoxyphenyl)vinyl]benzene from Step 1 above for 1-bromo-4-[2-(4-chlorophenyl)vinyl]benzene and performing the irradiation for 4 days.

후처리

  1. customthe irradiation for 4 days

출처 및 근거

ORD 기록
ord-bd83a9275f2e40258eb9bf809e9f8326
출처 데이터셋
uspto-grants-2011_05
특허 번호
US07943649B2

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