4-Methoxybenzohydrazide → 4-methyl-3-[4-(methyloxy)phenyl]-5-(4-penten-1-yl)-4H-1,2,4-triazole

반응식

[CH3:1][O:2][C:3]1[CH:12]=[CH:11][C:6]([C:7]([NH:9][NH2:10])=O)=[CH:5][CH:4]=1.Cl.[CH3:14][NH:15][C:16](=NC)[CH2:17][CH2:18][CH2:19][CH:20]=[CH2:21]>>[CH3:14][N:15]1[C:16]([CH2:17][CH2:18][CH2:19][CH:20]=[CH2:21])=[N:10][N:9]=[C:7]1[C:6]1[CH:11]=[CH:12][C:3]([O:2][CH3:1])=[CH:4][CH:5]=1

참가 물질

반응물 2

HCID 767924-Methoxybenzohydrazide

HCID 86630240N,N'-dimethyl-5-hexenimidamide hydrochloride

생성물 1

HCID 576919384-methyl-3-[4-(methyloxy)phenyl]-5-(4-penten-1-yl)-4H-1,2,4-triazole

실험 절차

The title compound was prepared in analogy to Preparation 11 in 0.12 g yield starting from 4-methoxybenzhydrazide (0.5 g) and N,N′-dimethyl-5-hexenimidamide hydrochloride (0.48 g). MS (m/z): 258 [MH]+.

후처리

customyield

출처 및 근거

ORD 기록: ord-dd747487230141da887e8c7b4864273f
출처 데이터셋: uspto-grants-2011_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07947683B2

반응 노트

불러오는 중…