Nitromethane → 2-Methyl-5-(2-nitro-vinyl)-thiophene

HRID 550615노트

반응식

HRID 550615 반응식
[CH3:1][C:2]1[S:6][C:5]([CH:7]=O)=[CH:4][CH:3]=1.[N+:9]([CH3:12])([O-:11])=[O:10]>>[CH3:1][C:2]1[S:6][C:5]([CH:7]=[CH:12][N+:9]([O-:11])=[O:10])=[CH:4][CH:3]=1

참가 물질

3

반응물 2

HCID 6375NitromethaneHCID 616635-Methyl-2-thiophenecarboxaldehyde

생성물 1

HCID 539158762-Methyl-5-(2-nitro-vinyl)-thiophene수율 76%

실험 절차

In close analogy to the procedure described above, 5-Methyl-thiophene-2-carbaldehyde is reacted with nitromethane to provide the title compound.

출처 및 근거

ORD 기록
ord-fc39b0f769304bca8773416015018713
출처 데이터셋
uspto-grants-2011_05
특허 번호
US07947689B2

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