Sodium triacetoxyborohydride → 4-Methyl-4,5,6,7-tetrahydrothieno[3,2-c]pyridine

HRID 550637노트

반응식

HRID 550637 반응식
[CH3:1][C:2]1[C:7]2[CH:8]=[CH:9][S:10][C:6]=2[CH2:5][CH2:4][N:3]=1.C(O[BH-](OC(=O)C)OC(=O)C)(=O)C.[Na+]>>[CH3:1][CH:2]1[C:7]2[CH:8]=[CH:9][S:10][C:6]=2[CH2:5][CH2:4][NH:3]1

참가 물질

3

반응물 2

HCID 5049666Sodium triacetoxyborohydrideHCID 218211774-methyl-6H,7H-thieno[3,2-c]pyridine

생성물 1

HCID 64852954-Methyl-4,5,6,7-tetrahydrothieno[3,2-c]pyridine수율 22%

실험 절차

In close analogy to the procedure described above, 4-Methyl-6,7-dihydro-thieno[3,2-c]pyridine is reacted with sodium triacetoxyborohydride to provide the title compound.

출처 및 근거

ORD 기록
ord-af25f08c80ae4b64a5ee2fa594a7b9fd
출처 데이터셋
uspto-grants-2011_05
특허 번호
US07947689B2

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