4-(2-Benzothiazol-2-ylthio)aniline → 1-[4-(2-Benzothiazolylthio)phenyl]-3-(4-chloro-3-trifluoromethylphenyl)thiourea

HRID 55083

반응식

HRID 55083 반응식
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][C:9]2[S:10][C:11]3[CH:17]=[CH:16][CH:15]=[CH:14][C:12]=3[N:13]=2)=[CH:4][CH:3]=1.[Cl:18][C:19]1[CH:24]=[CH:23][C:22]([N:25]=[C:26]=[S:27])=[CH:21][C:20]=1[C:28]([F:31])([F:30])[F:29]>>[S:10]1[C:11]2[CH:17]=[CH:16][CH:15]=[CH:14][C:12]=2[N:13]=[C:9]1[S:8][C:5]1[CH:4]=[CH:3][C:2]([NH:1][C:26]([NH:25][C:22]2[CH:23]=[CH:24][C:19]([Cl:18])=[C:20]([C:28]([F:31])([F:29])[F:30])[CH:21]=2)=[S:27])=[CH:7][CH:6]=1

참가 물질

3

반응물 2

HCID 1176104-(2-Benzothiazol-2-ylthio)anilineHCID 5200261-Chloro-4-isothiocyanato-2-(trifluoromethyl)benzene

생성물 1

HCID 189716771-[4-(2-Benzothiazolylthio)phenyl]-3-(4-chloro-3-trifluoromethylphenyl)thiourea

실험 절차

2-(4-Aminophenylthio)benzothiazole (10.0 moles, 2.6 g) and 4-chloro-3-trifluoromethylphenylisothiocyanate (10.0 moles, 2.4 g) were reacted according to procedure C to yield of the title compound, 1.5 g, 30%. Mass Spec (FD) 495. Calculated for C21H13ClF3N3S3 : C, 50.85 H, 2.64 N, 8.47. Found: C, 51.02; H, 2.71; N, 8.31.

출처 및 근거

ORD 기록
ord-6c4ba5c991764ddc92a5a0f1815b3425
출처 데이터셋
uspto-grants-1997_04
특허 번호
US05624937

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