Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(Trifluoromethyl)benzoic acid → 2-(Trifluoromethyl)benzoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(Trifluoromethyl)benzoic acid | HCID 9899 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 생성물 | 2-(Trifluoromethyl)benzoyl chloride | HCID 67561 | — |
반응 단계
A solution of 2.0 g of o-trifluoromethylbenzoic acid in 21 ml of thionyl chloride is heated at reflux for 1 hour. The volatiles are evaporated in vacuo to give a residue which is concentrated from toluene three times and dried under vacuum to give 2.1 g of the desired product as a residue.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05624923 |
| 출처 데이터셋 | uspto-grants-1997_04 |
| ORD ID | ord-c43ea7ec0d574071b997e0cd52b06fb1 |
| 출처 메모 | uspto-grants-1997_04 |