반응식
[C:1]1([CH3:11])[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[CH2:7][C:8](O)=[O:9].S(Cl)([Cl:14])=O>>[CH3:11][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[CH2:7][C:8]([Cl:14])=[O:9]참가 물질
3
실험 절차
A solution of 2.0 g of o-tolylacetic acid in 27 ml of thionyl chloride is heated at reflux for 1 hour. The volatiles are evaporated in vacuo to give a residue which is concentrated from toluene three times and dried under vacuum to give 2.1 g of the desired product as a light brown oil.
후처리
- temperatureat reflux for 1 hour
- customThe volatiles are evaporated in vacuo
- customto give a residue which
- concentrationis concentrated from toluene three times
- customdried under vacuum
출처 및 근거
- ORD 기록
- ord-9e3ada643d264e1abb01d8e9bf8ac9c6
- 출처 데이터셋
- uspto-grants-1997_04
- 특허 번호
- US05624923
연결된 노트
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