4-Chlorotoluene → Tris(4-methylphenyl)sulfanium Chloride
반응식
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([C:10]2[CH:15]=[CH:14][C:13]([CH3:16])=[CH:12][CH:11]=2)=O)=[CH:4][CH:3]=1.[Cl:17][C:18]1[CH:23]=[CH:22][C:21]([CH3:24])=[CH:20][CH:19]=1>O>[Cl-:17].[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([S+:8]([C:18]2[CH:23]=[CH:22][C:21]([CH3:24])=[CH:20][CH:19]=2)[C:10]2[CH:15]=[CH:14][C:13]([CH3:16])=[CH:12][CH:11]=2)=[CH:4][CH:3]=1참가 물질
4
실험 절차
The target compound was obtained by following the procedure of Synthesis Example 1 aside from using bis(4-methylphenyl)sulfoxide instead of the diphenyl sulfoxide and 4-chlorotoluene instead of the chlorobenzene in Synthesis Example 1, and increasing the amount of water for extraction.
후처리
- customThe target compound was obtained
- customthe procedure of Synthesis Example 1 aside
- customin Synthesis Example 1
- extractionfor extraction
출처 및 근거
- ORD 기록
- ord-72fe3b30ad0a48d78bceee8a6f63a51b
- 출처 데이터셋
- uspto-grants-2011_11
- 특허 번호
- US08048610B2
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