2-Naphthol → 9-(Naphthalen-2-yloxy)-3-aza-spiro[5.5]undecane

HRID 554474노트

반응식

HRID 554474 반응식
[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[OH:11].C(OC([N:19]1[CH2:24][CH2:23][C:22]2([CH2:29][CH2:28][CH:27](O)[CH2:26][CH2:25]2)[CH2:21][CH2:20]1)=O)(C)(C)C>>[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[O:11][CH:27]1[CH2:28][CH2:29][C:22]2([CH2:23][CH2:24][NH:19][CH2:20][CH2:21]2)[CH2:25][CH2:26]1

참가 물질

3

반응물 2

HCID 86632-NaphtholHCID 66701044tert-Butyl 9-hydroxy-3-azaspiro[5.5]undecane-3-carboxylate

생성물 1

HCID 160065489-(Naphthalen-2-yloxy)-3-aza-spiro[5.5]undecane

실험 절차

Was prepared according to method A from 2-naphthol and 9-hydroxy-3-aza-spiro[5.5]undecane-3-carboxylic acid tert-butyl ester. Mp. 132.2-133.8° C.

후처리

  1. customWas prepared

출처 및 근거

ORD 기록
ord-ceecfeb43dd2495cb156cf98f6f4237f
출처 데이터셋
uspto-grants-2011_11
특허 번호
US08049012B2

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