Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HCID 12660316, 화합물 → 2-Benzylphenol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | HCID 12660316 | HCID 12660316 | — |
| 촉매 | Palladium hydroxide | HCID 9942167 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 2-Benzylphenol | HCID 24216 | 67% |
반응 단계
To a solution of 2-(4-chlorobenzyl)phenol (618.5 mg, 2.83 mmol) in methanol (20 mL), a 20% palladium hydroxide catalyst (240 mg) was added. The mixture was stirred under a hydrogen atmosphere for three days, and then the catalyst was filtered off. The solvent was distilled under reduced pressure and the obtained residue was purified by silica gel column chromatography [developing solution=ethyl acetate:n-hexane (1:4)] to obtain the title compound (348.4 mg, 67%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08048897B2 |
| 출처 데이터셋 | uspto-grants-2011_11 |
| ORD ID | ord-882e0f4fdfcf4a8086b0b4f0864124f9 |
| 출처 메모 | uspto-grants-2011_11 |