N,N-Dimethyl-N-decylamine → HCID 86612068, 화합물

HRID 556253

반응식

HRID 556253 반응식
[CH:1]([C:3]1[CH:10]=[CH:9][C:6]([CH2:7][Cl:8])=[CH:5][CH:4]=1)=[CH2:2].[CH3:11][N:12]([CH3:23])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]>>[Cl-:8].[CH:1]([C:3]1[CH:10]=[CH:9][C:6]([CH2:7][N+:12]([CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])([CH3:11])[CH3:23])=[CH:5][CH:4]=1)=[CH2:2]

참가 물질

3

반응물 2

HCID 70711N,N-Dimethyl-N-decylamineHCID 74126p-Vinylbenzyl chloride

생성물 1

HCID 86612068HCID 86612068, 화합물

실험 절차

4-Vinylbenzyl chloride (18.60 g, 100 mmol) and N,N-dimethyl-N-decylamine (15.26 g, 100 mmol) were mixed in a 100 mL round bottomed flask. The mixture was allowed to sit overnight. The crystalline product was crushed and washed with ether. The product was collected by filtration (30.3 g, 90%)

후처리

  1. customThe crystalline product was crushed
  2. washwashed with ether
  3. filtrationThe product was collected by filtration (30.3 g, 90%)

출처 및 근거

ORD 기록
ord-d39455f6861e4af48fbccb83a3fd311d
출처 데이터셋
uspto-grants-2011_11
특허 번호
US08058208B2

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