Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl iodide → 3-Methoxy-2-nitropyridine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl iodide | HCID 6328 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 3-Hydroxy-2-nitropyridine | HCID 27057 | — |
| 생성물 | 3-Methoxy-2-nitropyridine | HCID 556063 | 97.4% |
반응 단계
The similar reaction as described in Reference Example 9 by using 2-nitro-3-hydroxypyridine (7.0 g), potassium carbonate (6.91 g) and methyl iodide (4.67 ml) gave the title compound (7.5 g) as crystalline powders.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08058280B2 |
| 출처 데이터셋 | uspto-grants-2011_11 |
| ORD ID | ord-756d09c03e2646658d6e0c70c3ed0126 |
| 출처 메모 | uspto-grants-2011_11 |