Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Bromobenzaldehyde → bis((E)-4-Bromostyrylsulfonyl)methane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Bromobenzaldehyde | HCID 70741 | — |
| 반응물 | Acetic acid, 2,2'-[methylenebis(sulfonyl)]bis- | HCID 2252641 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | bis((E)-4-Bromostyrylsulfonyl)methane | HCID 86619223 | 82% |
반응 단계
A solution of 4-bromobenzaldehyde (2 mmol) and carboxymethane-sulfonylmethanesulfonyl-acetic acid (1 mmol) in acetic acid (10 mL) was subjected to General Procedure 1, to yield the title compound in 82% yield. m.p. 213-215° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08058313B2 |
| 출처 데이터셋 | uspto-grants-2011_11 |
| ORD ID | ord-e9f6889bc79f4a22b2455d8601cacd6c |
| 출처 메모 | uspto-grants-2011_11 |