Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl iodide → 5-Fluoro-2,3-dimethyl-benzothiazol-3-ium iodide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl iodide | HCID 6328 | — |
| 반응물 | 5-Fluoro-2-methylbenzothiazole | HCID 597437 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 5-Fluoro-2,3-dimethyl-benzothiazol-3-ium iodide | HCID 66990784 | — |
반응 단계
13.0 g (10.4 ml, 77.7 mmol) 5-Fluoro-2-methyl-benzothiazole and 22.1 g (9.47 ml, 156 mmol) iodomethane were boiled in ethanol for 7 h. The residue was filtrated. 4.00 g=17% white powder
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08058431B2 |
| 출처 데이터셋 | uspto-grants-2011_11 |
| ORD ID | ord-ca4303ac31c042c0bca4858ea5b4ad7a |
| 출처 메모 | uspto-grants-2011_11 |