Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydroxylamine → N'-hydroxy-2-phenylethanimidamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydroxylamine | HCID 787 | — |
| 반응물 | Phenylacetonitrile | HCID 8794 | — |
| 반응물 | N'-Hydroxybenzenecarboximidamide | HCID 69186 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | N'-hydroxy-2-phenylethanimidamide | HCID 2731007 | 81.9% |
반응 단계
Benzyl cyanide (1 g, 8.5 mmol) and hydroxylamine (50% in water, 1.04 cm3, 17 mmol, 2 eq) in EtOH (8.5 cm3) were reacted in the same manner as in the preparation of N′-hydroxybenzimidamide (EtOAc used in extraction) to give the product N′-hydroxy-2-phenylacetimidamide (1.04 g, 81.9%) as a pale yellow solid, mp 63.5-64.5° C. (lit 57-59° C.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08062429B2 |
| 출처 데이터셋 | uspto-grants-2011_11 |
| ORD ID | ord-7126ea936ddf4af08606b069eb5d41bb |
| 출처 메모 | uspto-grants-2011_11 |