Water → Ar,ar-dinitrobenzenamine
반응식
[N+:1]([C:4]1[C:9]([N+:10]([O-:12])=[O:11])=[CH:8][CH:7]=[CH:6][C:5]=1[NH:13]C(=O)C)([O-:3])=[O:2].C[O-].[Na+].O>CO>[N+:1]([C:4]1[C:9]([N+:10]([O-:12])=[O:11])=[CH:8][CH:7]=[CH:6][C:5]=1[NH2:13])([O-:3])=[O:2]참가 물질
5
실험 절차
To a solution of N-(2,3-dinitrophenyl)acetamide (3.0 g) in methanol (200 mL) was added sodium methoxide (72 mg). The stirred solution was heated at reflux for 3 hours. Water was added to the solution (300 mL) and the yellow solid precipitate was collected and dried to give the desired product (2.27 g, 93%). Chemical Formula: C6H5N3O4 Molecular Weight: 183.12; MS (ES) m/z 184
후처리
- temperatureThe stirred solution was heated
- temperatureat reflux for 3 hours
- customthe yellow solid precipitate was collected
- customdried
출처 및 근거
- ORD 기록
- ord-d43da1a7075a443abe0771762c7104a4
- 출처 데이터셋
- uspto-grants-2011_11
- 특허 번호
- US08063053B2
반응 노트
불러오는 중…