Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Acid → N'-(4-Iodophenyl)acetohydrazide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Acid | HCID 176 | — |
| 반응물 | 4-Iodophenylhydrazine | HCID 704591 | — |
| 생성물 | N'-(4-Iodophenyl)acetohydrazide | HCID 623860 | — |
반응 단계
A mixture of 10 g of 4-iodophenylhydrazine in 80 ml of acetic acid is refluxed for 5 hours. The reaction mixture is concentrated under vacuum, the residue is taken up with water, and the precipitate formed is filter-dried and washed with a propan-2-ol/PE (50/50; v/v) mixture. 9 g of the expected compound are obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08063061B2 |
| 출처 데이터셋 | uspto-grants-2011_11 |
| ORD ID | ord-bc6017e9c2914504b8961b1c59b6217f |
| 출처 메모 | uspto-grants-2011_11 |