Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,3-Dimethyl-5-nitroisoquinoline → 1,3-Dimethylisoquinolin-5-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,3-Dimethyl-5-nitroisoquinoline | HCID 57456780 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 1,3-Dimethylisoquinolin-5-amine | HCID 22337624 | — |
반응 단계
A solution of D3 (2.01 g, 9.94 mM) and 10% palladium on charcoal (1 g) in methanol was hydrogenated at atmospheric pressure for 1 h. The catalyst was filtered off and the filtrate concentrated under reduced pressure to afford the title compound as an off white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08063078B2 |
| 출처 데이터셋 | uspto-grants-2011_11 |
| ORD ID | ord-8b298f91f862430fb1b4d0d9f7fe359c |
| 출처 메모 | uspto-grants-2011_11 |