Methyl 3-oxo-3,4-dihydro-2H-1,4-benzoxazine-8-carboxylate → 3-oxo-3,4-dihydro-2H-1,4-benzoxazine-8-carboxylic acid

HRID 560279노트

반응식

HRID 560279 반응식

C[O:2][C:3]([C:5]1[C:14]2[O:13][CH2:12][C:11](=[O:15])[NH:10][C:9]=2[CH:8]=[CH:7][CH:6]=1)=[O:4]>CC#N>[O:15]=[C:11]1[NH:10][C:9]2[CH:8]=[CH:7][CH:6]=[C:5]([C:3]([OH:4])=[O:2])[C:14]=2[O:13][CH2:12]1

참가 물질

3

반응물 1

HCID 23770643Methyl 3-oxo-3,4-dihydro-2H-1,4-benzoxazine-8-carboxylate

생성물 1

HCID 183549413-oxo-3,4-dihydro-2H-1,4-benzoxazine-8-carboxylic acid

시약·촉매·용매 1

HCID 6342Acetonitrile용매

실험 절차

prepared by saponification of 3-oxo-3,4-dihydro-2H-benzo[1,4]oxazine-8-carboxylic acid methyl ester. LC-MS: tR=0.56 min; [M+CH3CN+H]+=235.0.

출처 및 근거

ORD 기록: ord-1313ecd0d47b46e08132f83b6a7ed2a4
출처 데이터셋: uspto-grants-2011_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08063099B2

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