Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzylamine → Ethyl 3-(benzylamino)-3-methylbutanoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzylamine | HCID 7504 | — |
| 반응물 | Ethyl 3,3-dimethylacrylate | HCID 12516 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Ethyl 3-(benzylamino)-3-methylbutanoate | HCID 288946 | 21.1% |
반응 단계
A solution of ethyl 3,3-dimethylacrylate (19.3 g, 0.151 mol) in EtOH (150 mL) was added benzylamine (16.2 g, 0.151 mol) and refluxed for 24 h. The reaction mixture was concentrated in vacuo. The distillation of the residue gave ethyl 3-benzylamino-3-methylbutyrate as a colorless oil (7.48 g, 21%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08063221B2 |
| 출처 데이터셋 | uspto-grants-2011_11 |
| ORD ID | ord-319b932dd8ae4c888979a6e751abcd91 |
| 출처 메모 | uspto-grants-2011_11 |