Potassium Carbonate → HCID 22467254, 화합물

HRID 561793노트

반응식

HRID 561793 반응식
C([C:3]1[C:8]([CH3:9])=[C:7]([Cl:10])[CH:6]=[CH:5][C:4]=1[OH:11])C.C(=O)([O-])[O-].[K+].[K+].Br[CH2:19][CH2:20][O:21][CH3:22]>CC(C)=O>[Cl:10][C:7]1[CH:6]=[CH:5][C:4]([O:11][CH2:19][CH2:20][O:21][CH3:22])=[CH:3][C:8]=1[CH3:9]

참가 물질

5

반응물 3

HCID 11430Potassium CarbonateHCID 809722-Bromoethyl methyl etherHCID 22134509Ethyl 4-chloro-3-methylphenol

생성물 1

HCID 22467254HCID 22467254, 화합물

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

To a solution of ethyl 4-chloro-3-methylphenol (1 eq.) in acetone (0.2 M) was added potassium carbonate (5 eq.) and 1-bromo-2-methoxyethane (1.3 eq.). The resulting suspension was refluxed for 25 h. The insolubles were removed via filtration and the filtrate was concentrated in vacuo to furnish the title compound.

후처리

  1. temperatureThe resulting suspension was refluxed for 25 h
  2. customThe insolubles were removed via filtration
  3. concentrationthe filtrate was concentrated in vacuo

출처 및 근거

ORD 기록
ord-224af951c7104183870510e77339fa69
출처 데이터셋
uspto-grants-2011_11
특허 번호
US08063105B2

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