Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl cyanoacetate → Poly(oxy-1,2-ethanediyl), alpha-[4-(2-cyano-3-ethoxy-3-oxo-1-propenyl)phenyl]-omega-hydroxy-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl cyanoacetate | HCID 7764 | — |
| 반응물 | Hexane | HCID 8058 | — |
| 반응물 | Benzaldehyde, 4-(2-hydroxyethoxy)- | HCID 89178 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Poly(oxy-1,2-ethanediyl), alpha-[4-(2-cyano-3-ethoxy-3-oxo-1-propenyl)phenyl]-omega-hydroxy- | HCID 50742116 | — |
반응 단계
Ethyl cyanoacetate (1.1 eq.) and 4-(2-hydroxyethoxy)benzaldehyde (1 eq.) were combined in ethanol (1.2 M). The reaction mixture was stirred at RT for 48. To this was then added an equal volume of hexane and the title compound was isolated by filtration as a pale yellow solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08063105B2 |
| 출처 데이터셋 | uspto-grants-2011_11 |
| ORD ID | ord-1040e73697ea45ebbefdd1e7f8935a97 |
| 출처 메모 | uspto-grants-2011_11 |