참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2-Furanpropionic acid | HCID 70286 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 3-(Oxolan-2-yl)propanoic acid | HCID 263161 | — |
반응 단계
A mixture of 3-(furan-2-yl)propanoic acid (11.0 g, 80.0 mmol) and Pd/C (1.1 g, 10%) in MeOH (110 mL) was stirred at 60° C. under 30 bar of H2 overnight. The mixture was then filtered and the filtrate was concentrated in vacuo to give the title compound, which was used for next step without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US09434695B2 |
|---|
| 출처 데이터셋 | uspto-grants-2016_09 |
|---|
| ORD ID | ord-9f3c11f0258740c08bd5d0b5b6d2e178 |
|---|
| 출처 메모 | uspto-grants-2016_09 |
|---|
