Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sulfur dichloride → 3-(3-Fluorophenyl)propanoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sulfur dichloride | HCID 25353 | — |
| 반응물 | 3-(3-Fluorophenyl)propionic acid | HCID 2737489 | — |
| 생성물 | 3-(3-Fluorophenyl)propanoyl chloride | HCID 18993501 | — |
반응 단계
A mixture of 3-(3-fluorophenyl)propanoic acid (2.50 g, 14.9 mmol) and dichlorosulfane (10 mL) under N2 was refluxed for 3 h. The mixture was cooled to rt and concentrated in vacuo to give the title compound, which was used for next step without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09434695B2 |
| 출처 데이터셋 | uspto-grants-2016_09 |
| ORD ID | ord-119617a6c7804e7aa0f70ecb08b9ebb9 |
| 출처 메모 | uspto-grants-2016_09 |