Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sulfur dichloride → 4-(3-Fluorophenoxy)butanoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sulfur dichloride | HCID 25353 | — |
| 반응물 | 4-(3-Fluorophenoxy)butanoic acid | HCID 6486015 | — |
| 생성물 | 4-(3-Fluorophenoxy)butanoyl chloride | HCID 90023167 | — |
반응 단계
A solution of 4-(3-fluorophenoxy)butanoic acid (3.00 g, 15.1 mmol) in dichlorosulfane (15 mL) under N2 was refluxed for 3 h. The mixture was cooled to rt and concentrated in vacuo to give the title compound, which was used for next step without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09434695B2 |
| 출처 데이터셋 | uspto-grants-2016_09 |
| ORD ID | ord-f4e72ac7cd384758b6534f103e26e766 |
| 출처 메모 | uspto-grants-2016_09 |