Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sulfur dichloride → 2-(Cyclohexyloxy)acetyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sulfur dichloride | HCID 25353 | — |
| 반응물 | Cyclohexoxyacetic acid | HCID 191994 | — |
| 생성물 | 2-(Cyclohexyloxy)acetyl chloride | HCID 12484123 | — |
반응 단계
A mixture of 2-(cyclohexyloxy)acetic acid (0.90 g, 5.69 mmol) and dichlorosulfane (10 mL) was refluxed for 2 h. The mixture was cooled to rt and concentrated in vacuo to give the title compound as yellow oil, which was used for next step without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09434695B2 |
| 출처 데이터셋 | uspto-grants-2016_09 |
| ORD ID | ord-8af8cc706d3a457badbaab90d0f5f777 |
| 출처 메모 | uspto-grants-2016_09 |