Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Nitrogen → 2-(3-Fluorophenoxy)-2-methylpropanoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Nitrogen | HCID 947 | — |
| 반응물 | Sulfur dichloride | HCID 25353 | — |
| 반응물 | 2-(3-fluorophenoxy)-2-methylPropanoic acid | HCID 22270720 | — |
| 생성물 | 2-(3-Fluorophenoxy)-2-methylpropanoyl chloride | HCID 82113850 | — |
반응 단계
To 2-(3-fluorophenoxy)-2-methylpropanoic acid (1.70 g, 8.58 mmol) was added dichlorosulfane (15 mL) dropwise under N2 and the mixture was refluxed for 3 h. The mixture was cooled to rt and concentrated in vacuo to give the title compound as yellow oil, which was used for next step without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09434695B2 |
| 출처 데이터셋 | uspto-grants-2016_09 |
| ORD ID | ord-9e3a5970c34243519043534d48bb17a0 |
| 출처 메모 | uspto-grants-2016_09 |